| 液态金属X射线衍射仪
Liquid metal X-ray diffractometer consists of three parts:
X-ray collection system、vacuum and atmosphere protecting system、specimen
heating and moving system、automation system. The X-ray diffraction
was carried out adopting q-q type. Measurements were carried
out in high purity helium atmosphere before the chamber was
cleaned by vacuum equipment. Specimens were placed in an alumina
crucible, and were heated by a pair of Ta sheets. Mo Ka radiation
was reflected from the free surface of the liquid specimen,
the X-ray then reached the detector through a graphite monochromator
in the diffraction beam. During the measurements, the surface
of the specimen was fixed to one horizontal position by means
of a laser calibrator. The Diffraction X-ray scattering intensity
measured in arbitrary units can be converted into the coherent
scattering intensity per atom in an electron unit. Structure
factors、pair correlation functions、coordination number、nearest
neighbor distance and so on, can be obtained by calculation
and analysis of experimental datum.
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